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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018542
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 1-Monolinoleoylglycerol trimet Concentration Rank 12

R.T. EstCono Area Relative to ISTD R.T.

36.72 3.56 ug/1 917056 Perylene-d12 37.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 39 2 Propanoic acid,2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 25 3 Propanedioi acid, bis (trimethylsil 248 C9H20O4Si2 018457-04-0 25

X_ 4 Ethanedioid acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 Abundance Scan 3450 (36.720 mln): 28323.D (-) m/z 73.Q0 100.00% 73

147 5000

m/z ".TT 221 281 355 ’’ j 1 i-rr| r 1 1 1 । i m 1» rr . t 429 36.40 36.60 36.80 37.00 44 • 1 l 1 ■ 96 117 —PT A < ■ 1914 —249.432744401 -- miz-> 50 100 150 200I 250 300 350 400 450 Abundance #58871:1-Mondinoleoylglycerol trimethylsilyl ether 73

207 5000 147 36.40 36.60 36.80 37.00 34 103 281 m/z 221.05 35.63% | 395 20101/010000011/11211111- 482 '450 ' ' ‘ m/z-> 50 100 150 200 250 ___300 350 400 Abundance #30222. Przpanoic acid. 2-or mmetle ’silyl), mmethy 147 73 1 1 1 ' 1 1 1 I 1 1 ' 1 I ‘T ‘ ' I TTT 36.40 36.60 36.80 37.00 5000 m/z 281.00 19.32% 45 217 117, , 189 |.................................... ................................. 50 100 ' 150 m/z-> 200 250 300 350 400 450 Abundance #33321: Propanedioic acid, bis(trimethylsilyl) ester 147 36.40 36.60 36.80 37.00 73 m/z 207.00 15.62% 5000-

45 233 117 — Ji . . . 204 .. .......................................... ■ 1 I 1 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ 1 i • • ■ ■ i m/z-> 50 ' 100 ' ' 150 200 250 300 350 400 450 36.40 36.60 36.80 37.00

28323.D GCMS1126.M Wed Feb 06 13:02:46 2002 Page 18

NYC-WTC_000018542

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NYC-WTC_000018542Source: NYC Law Department, mirrored locally

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