GCMS analysis results for sample AD30426, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.49 ug/1 315476 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 23 Abundance Scan 3326 (35.575 min): 30426.D (-) m/ z 73.0.0 100.00% 73

147 5000 221 281 355 • l ‘ • r1 | . l . | I 35.20 35.40 35.60 35.80 36.00

m/z~> 40 , r f ‘n f 50 96 117 100 .18514 150 200 249 250 13274414 300 350 400 450 m/z 147.00 51.09% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 r PPI 11 meen 1- 5000 147 35.20 35.40 35.60 35.80 36.00 34 103 m/z 221.05 31.72% ... . . . ।! 281 । 395 482 350 400 ’450' ’ m/z-> 50 100 150 ' 200 250 300 Abundance #74103; Trisiloxane, 1,1.1.5,5,5-hexamethy-3,3-bis[{trimet 73 147 • i • * • • I 35.20 35.40 35.60 35.80 36.00 5000 m/z 281.00 18.50% 281 45 369 117 207 249 | *44 1 41*1* m/z-> 50 100 150 200 250 300 350 400 450 Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester * 1 i • 73 35.20 35.40 35.60 35.80 36.00 m/z 355.05 15.66% 147 5000

45 1. I 190 219 * • i • ' 117 — ■ i ■ ' 1 r i ' 1 1 ' i ■ 1 ' 1 i • * i • m/z-> 50 '160' ' 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80 36.00

30426.D GCMS1126.M Wed Jan 02 11:08:34 2002 Page 13

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