GCMS analysis results for sample AD30426, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

38.02 0.49 ug/1 103388 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 4 Ethanimidic acid, N-(trimethylsilyl 203 C8H21NOS12 010416-59-8 12 Abundance Scan 3592 (38.017 min): 30426.D (-) m/ z 73.00 100.00% 73

147 5000 221 281 355 i • ■ 1 • i ■ • • • i ■ ■ ■ ■ i ■ ■ • ‘ i 1 ■

191, t 253, | , 429 37.60 37.80 38.00 38.20 38.40 ■ 45 pi r"i 105 T’Tr—Hr । ‘ 1 । • • • ■ । ■ ■ f ■ i ■ ■ • ‘ । _L ■ i ■ mmmmm m/z 147.00 51.95% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoyiglycerol trimethylsilyl ether

.Y 73

207 5000 147 37.60 37.80 38.00 38.20 38.40 34 103 i 281 m/z "

m/z~> 50 100 150 200 1 .X 482. 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1.1.1.7.7.7-bexamethyl-3,5,5-trs(trim 73 i....... 1 ■ Y ‘ ‘ • i • • 37.60 37.80 38.00 38.20 38.40 5000 m/z 281.00 20.54%

m/z-> Abundance 50

73 100 147

■ ■ i ■ ■ ■ 1 i • ■ • ■ i • • ■ • i • • ■ ‘ । 1 1 ' ■ i ■ ■ ' 1 i ■ ■ ■ ■ i • ' ■ ■ i ■ • • * i ■1 ■ ■ । 1 ■ 150 #30949: Mercaptoacetic acid, bis(trimethyisily!)- 147 200 221

250 281

300 327

350 400 415 450 500 519 561 550 _X_ T 37.60 37.80 38.00 38.20 38.40 m/z 207.00 14.67% 188

" "" 5000 221 45 104 193 ‘ 1 I 1 ‘ ■ i ■ ■ ■ ' 1 1 • ■ ■ i 1 • ‘ 1 I ■ f' 1 i 1 1 ' 1 i ' ' miz-> 50 100 150 200 250 300 350 400 450 500 550 37.60 37.80 38.00 38.20 38.40

30426.D GCMS1126.M Wed Jan 02 11:08:43 2002 Page 15

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