Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L • ********************************************************************* Peak Number 16 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.
34.37 5.17 ug/1 1814650 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------- ------------------------------------------------------------------------------------- 1 3-Isopropoxy-1.1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 9,12,15-9ctadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 23 Abundance Scan 3194 (34.370 min): 28323.D (-) m/ z 100.00% 73
5000 147 221 T-T-r-r 14 1’’ V' l 1 281 355 34.00 34.20 34.40 34.60 34.80 45 117 TTTT TTTT 4 ■ . 1911 k 251- i 327, 1 401 429 f i L| । i fint TTIPIOT m/z 147.00 47.42% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 —. er -i ■. ni 1 T-r-r-r-n-r-j-T 147 34.00 34.20 34.40 34.60 34.80
221 281 m/z 221.05 26.85% 327 415 519 561 ■ ■ i • • ■ 1 i 1 ■ ‘ • i ■ ■ ■ 1 i ■ ■ ■ ■ i ‘ — 1 ■ i ■ '■ ■ ■ i • ■ • ‘ i •‘ 1 i ' ■ ‘ ■ i mfz~>50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1.Merclinolepviglycerci trimejiysilvi her 73 ' l » • • ‘ l ‘ 34.00 34.20 34.40 34.60 34.80 207 .5000 147 / 34 103 281 -------------------------------------------------------- 395....482 ...... miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester 11 TTIm 73 34.00 34.20 34.40 34.60 34.80 m/z 355.0 14.53% 147 5000
45 1. ■ 117 190 219 ........... miz-> 50 100 150 ' ‘ 200 ' ‘ 250 ' 300 ' ' 350 ' ' 400 ' 450 ' 500 550 34.00 34.20 34.40 34.60 34.80
28323.D GCMS1126.M Wed Feb 06 13:02:36 2002 Page 16
NYC-WTC_000018540
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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