Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018546–000018575Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 34.37 0.29 ug/1 117779 Chrysene-dl2 33.02
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropox/-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 3 2-Hexenedioic acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 3195 (34.373 min): 30706.D (-) m/ z 73.00 100.00% t 73
5000 147 221 CIT ---PPP= 281 355 44 Pt 4 14117,4.. , 327, I 11—, r 401 429 34.00 34.20 34.40 34.60 34.80 m/z 147.00 44.67% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 1 1 1 ■ 1 1 । ■ 1 ' ■ i 1 1 । 1 1। ' ■ 147 34.00 34.20 34.40 34.60 34.80 m/z 221.0,5 26.21% .............................. 327, 415 , 519561 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.00 18.00% 45 117 1.. 190 219 ......... ............................................................ miz-> 50 100 150 200 250 ’300 350 400 450 500 550 A4A4—444*,YM4RAA Abundance #40777:2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- 73 34.00 34.20 34.40 34.60 34.80 'm/z 355.0 14.75% 5000 147 45
m/z-> — 50 41. 100 244 273 ' I 1 1 ' 150 200 250 300 350 400 450 i ' ' ' ‘ i ‘ ‘ i ‘ ‘ ‘ ‘ i ‘ ‘ ‘ ' i ‘ ‘ ‘ ■ i ' ‘ ‘ ' i ‘ ‘ 500 550 34.00 34.20 34.40 34.60 34.80
30706.D GCMS1126.M Fri Feb 01 11:08:53 2002 Page 14
NYC-WTC_000018574
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NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
Filed in the same folder
NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder