DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.71 1.87 ug/1 720097 Chrysene-dl2 33.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 2-Hexenedioic acid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23 4 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 Abundance Scan 2905 (31.714 min): 30641 .D (-) m/z 73.00 .. 100.00% 73

5000 147 221 I 281 255 I , 325 [ 1911.251 401 429 31.40 31.60 31.80 32.00 45 117.. , I l rh-mmim 1*1 ril, ' ■'I 1 r I "11“ 1 I I f fl H I I I I I I I PImp m/z 147.00 40.03% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim

5000 73

147 ... a.... 31.40 31.60 31.80 32.00 m/z 221.05 23.90% I 221 21 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777 2-Hexencdlolc acid, is(trimethylsily!) ester, (E)- 73

31.40 31.60 31.80 32.00 5000 m/z 281.00 15.18% 147 45 i 112 244 273 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester i 73 147 31.40 31.60 31.80 32.00 m/z 355.05 . 11.35% 5000 45

, J, 111, , 190 219 .............. m/z-> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00

30641.D GCMS1126.M Mon Jan 28 11:14:28 2002 Page 11

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