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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004426
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglyeerol trimet Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

34.38 1.33 ug/1 511909 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglyeerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 dl -Xyl itol, cyclic 2,3- (phenylboron 238 C11H15BO5 074793-46-7 27 Abundance Scan 3195 (34.377 min): 30641 .D (-) m/z " 100.00% 73

147 5000 221 281 355 34.00 34.20 34.40 34.60 34.80 45 ............. 2494 4,4.3271., 401.429 m/z 147.00 50.99% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 i 207 5000 147 1 IPI-PI 1111 1Ti * 1 ■ > i 1 34.00 34.20 34.40 34.60 34.80 34 103 ; 281 m/z 221.05 30.25% -

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #80503: 3-Isopropoxy-1.1,1.7.1.7 buxamethvi-3 5 5-iris(trim 73 111111 ' ' I ' ' ' ' I ' 34.00 34.20 34.40 34.60 34.80 5000- m/z 281.00 17.32% 147 221 281 207 AE ’ । 54 415 519 561 m/z-> (Abundance 50 100 150 200 250 300 350 400 #30580: Ethanedioic acid, bis(trimethylsiiyl) ester 450 500 550 IT 73 147 34.00 34.20 34.40 34.60 34.80 m/ Z 355.05 16.83% 5000 45 190 219 , . ill T 1 1 1 1 - m m/z-> 50 100 150 200 250 300 350 400 450 500 550 34.00 34.20 34.40 34.60 34.80

30641.D GCMS1126.M Mon Jan 28 11:14:32 2002 Page 12

NYC-WTC_000004426

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NYC-WTC_000004426Source: NYC Law Department, mirrored locally

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