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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004424
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

30.25 2.12 ug/1 815568 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2,4 -bis [ (trimethylsil 370 C16H3004Si3 010586-16-0 30 2 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 30 3 3-Isopropoxy-1,1,1, 7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Silanamine, N-42,6-dimethyl-4 -[(tri 281 C14H27NOSi2 _072088-09-6 22 Abundance 73 Scan 2745 (30.246 min): 30641 .D (-) m/z 73.00 100.00%

5000 147 221 1I ITT 1 1 1 1 1 1 1 1 1 I 281 355 429 30.00 30.20 30.40 30.60

m/z~> 45 -1— ' '5 1 1 50 150 100 191 .249, 1, 327, I, . 401 . ...... 200 250 300 350 400 450 500 550 m/Z 147.00 35.11% Abundance #73975; Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

5000 355 ' 1 1 1 1 T 1 N ' ' ■ I ' ’ 30.00 30.20 30.40 30.60 45 m/z 221.05 20.11% i 133 193 223 281 I m/Z“> 50 100 150 200 250 300 350 400 450 500 550 Abundance 5714; 1.1.1.57.7.7 Heotamethyl-,3-bstirimethylsiloxy)t 73 1 ' i ■ ' y... 30.00 30.20 30.40 30.60 147 5000 267 m/z 355.05 13.00% 355 429 45 207

m/z--> Abundance 50 73 100__ 150__ 200__ 250__ 300__ 350__ 400 450 #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyi-3,5,5-tris(trim 500 550 .. A.. 30.00 30.20 30.40 30.60 m/z 281.00 12.44% 5000 147 221 21 327 415 519 561 "tIT ’ T’IIIII" miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60

30641.D GCMS1126.M Mon Jan 28 11:14:23 2002 Page 10

NYC-WTC_000004424

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NYC-WTC_000004424Source: NYC Law Department, mirrored locally

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