GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 30.25 1.82 ug/1 487401 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 28 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27 41,1,1,5,7,7,7-Heptamethyl-3,3-bis(t444C13H4005Si6 038147-00-1 23 Abundance 7(3 7 m/z 72.9,5 100.00% Scan 2745 (30.246 mln): 30256.D (-)

5000 147 (J l y I I I ill 4 221 1II 281 I 355 1914——249443274 401 429 45 30.00 30.20 30.40 30.60 117 . nine r.-. । i" fi >»* r1 * i * ’ > * i * * * * i ’ • m/z 147.00 35.48% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ‘1** • ‘ I ' ‘ 147 30.00 30.20 30.40 30,60 221 281 M7 ... m/z 221.0 20.12% । [ ( 327, । i i i i । 415 i । । i | > r i i | i । r i । i i 'h i 519i i ।561 i i । i i i > ]■ i r i m/z-> 50 100 150 200 250 300 350 400 450 500 550 {Abundance #58871: 1-Monolinoleoyiglycerol trimethylsilyl ether 73 TTI T 207 30.00 30.20 30.40 30.60 5000 147 m/z 281.00 12.73% 34 103 281

1 395 482 *4*/*a//a//aaaana414*Iaa/n/a*Ia**Ia***IF*IIIBIIIIII miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]- trimet T I ' ‘ ‘ ’ 1 58. 73 30.00 30.20 30.40 30.60 m/z 355.05 11.83% 5000 355 45

j [..... 133 193 223 ,281 ..... I......................... miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60

30256.D GCMS1126.M Wed Jan 02 10:24:58 2002 Page 11

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