GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.71 1.61 ug/1 430423 Chrysene-dl2 33.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 4 Butanoic acid,/3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 2905 (31.715 mln): 30256.D (-) m/z 73.0,0 100.00% 73

5000 147 221 281 355 290 31.40 31.60 31.80 32.00UT miz—> 45 I 1 1 50 100 194 150 200 249. [ . 327, [ 117 401 429 250 300 350 400 450 500 550 i r" Pihy 1 **|h 1 j■ i | i "i r i j it > । । 1 i i i ] ii m/z 147.00 39.60% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 31.40 31.60 31.80 32.00 34 103 i 281 m/z 221.05 22.71% ............... .................. .......................................... m/z-> 50 100 150200 250 300 350 400 450 500 550 Abundance 50503: 3-Isoprepoxv-'. 1.1.7,7,7-hexamethy/-3,5,5-tris(trim 73

31.40 31.60 31.80 32.00 5000 m/z 281." 14.37% 147

1 221 281 327 ■ ■ i ■ ■ ■ 1 i 1 ' 1 r I ' ' 1 1 I 1 f 1 1 1 1 1 ' ■ j ' ' 1 1 i • ‘ 415 ■ I ■ 1 • ' i ■ ■ 1 ■ i 519 ■ > । 561 m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bis(trimethylsllyl) ester, (E)- r‘ । • • • • । * * • * r * * * * । * * * ‘ i 73 31.40 31.60 31.80 32.00 m/z 207.0,0 10.23% 5000 147 45 244 273 TTTH ‘ * I112 ‘ ' ■ ■ I ■ ■ • • t ■ ■ 1 •' i • ‘ ■ • i ‘ ' i ■ ' ■ 1 i ‘ ‘ ‘ ■ i ■ ' ' ■ i ■ ‘ 1 ‘ i ' ‘ । » j n j » [ » । i » 1171" r i । i j i i । m/z-> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00

30256.D GCMS1126.M Wed Jan 02 10:25:03 2002 Page 12

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