GC/MS calibration data for sample 28322, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 8

R.T. EstCoric Area Relative to ISTD R.T.

31.71 3.41 ug/1 1146180 Chrysene-dl2 33.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 3-Isopropoxy-l,l,l,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 32 4 2-Hexenedioic acid, his(trimethylsi 288 C12H2404Si2 055494-10-5 23 Abundance 73 Scan 2905 (31.714 min): 28322.D (-) m/z 73.00 ’ 100.00%

5000 147 221 249 , 281 1 , 327 255 1 401 429 31.40 31.60 31.80 32.00 mlz-> 45 117 TTT TTTd 50 100 150 200 +1914 — I I r4 Pe **[0214**12/012/* 250 300 350 400 450 500 550 m/z 147.00 41.84% Abundance #58871:1-Monoiinoleoylglycerol trimethylsily ether 73 207 5000 147 1 "111 ■ 1 ■ i11 ■ n ’1 111111 1 i 31.40 31.60 31.80 32.00 34 103 . m/z 221.05 23.43% 281 395 I .... T-Edn/11*11r11111t11111183 482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 .1.1,7. /-hoxamethy!-3,5,6-tris(trim 73

31.40 31.60 31.80 32.00 ' ' ‘ 5000 m/z 281.0,0 15.58% 147 221 281 327 415 519 561 1' t1 ■' ■ ।'1 ■11 • ■1 FT •1' । •1 ■' i ■1 ■■11 ■ ■ ■ ■ i' ■' ■111 * ■ • । ■1 • ■ । ■' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedioic acid, bls(trimethylsilyl) ester 73 31.40 31.60 31.80 32.00 ‘ m/z 355.0,5 11.61% 147 5000

45

miz-> —4 -1--= 50 190 219 .............. ' I 1 1 ' 1 I 1 ' 1 1 I ■ ■ ■ ‘ i ■ ■ 1 ‘ i • ‘ 100 150 200 250 300 350 400 450 500 550 ■ i ‘ ‘ • i ' ■ ■ ■ I ■ ■ ■ ■ I 1 ■ ■ ■1 ■ • ■ ■ i • ■ ■ ■ i 31.40 31.60 31.80 32.00

28322.D GCMS1126.M Wed Feb 06 12:56:42 2002 Page 14

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