Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018492–000018518Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.24 3.78 ug/1 1272230 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 33 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 32 3 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 Abundance Scan 2745 (30.245 min): 28322.D (-) m/ z 73.0,0 100.00% 73
5000 147 221 IIIFTT 1 i ■ ' ' ■ i 1 ‘ 281 327 355 383401 42% 30.00 30.20 30.40 30.60 45 .1 96 117 165 191 L 249 , L , mpfo TTTTTTT tm TTTMTTTmp m/z 147.00 37.10% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 • • i • • 5000 267 ' ■ i ■ ‘ 30.00 30.20 30.40 30.60 ‘ I ' ' 355 429 45 207 i m/z 221.05 22.01% “ “ I ‘121141 TIumnmnmmmuCe—mnmmnmuIEOTT | ... । |H | | . . 11 । . Wz-> 40 60 80 10012014016018020022024026028030032 0340360380400420 Abundance #52459; Trisiloxane 1.1.1.5 6.5hexamelly-3.3-bis[tirmet 73 147 281 30.00 30.20 30.40 30.60 5000 m/z 355.0 13.43%
: on? 369 207 249. ..... 338.. ,....... 1 I1.... IH..1.... J.... 1....11|J|1.A.I .... 11 I I I11 1111 ■ mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-{(trimethylsilyl)oxyJ • ■ i • ■ ■ i ■ ■ ■ ■ i ■ • 73 30.00 30.20 30.40 30.60 281 m/z 281.00 12.79% 209 5000 45 251 179 125 147 miz-> 7111*1mmmml TTTp 11 n 111 > il 11 ? ।,... ।.... (. 111,.., ।..,.!..., 11,., t.... ।. 40 60 80 100120140160180 200 220 240260 280 300 320 340 360 380400420 * ■ । • 30.00 30.20 30.40 30.60
• 28322.D GCMS1126.M Wed Feb 06 12:56:37 2002 Page 13
NYC-WTC_0000 18510
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NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018416
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NYC-WTC_000018420
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