DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

33.08 2.75 ug/1 1083680 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 17 3 N-(Trifluoroacetyl)-0,OO'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 14 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2____ 072088-09-6 12 Abundance Scan 3054 (33.084 min): 30707.D (-) m/z 73.0.0 100.00% 73

5000 147 221 281 355 32.80 33.00 33.20 33.40 45 TTTT I 117 4, 191, , +24944325,4401_ m/z " 46.73% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 32.80 33.00 33.20 33.40 m/Z 221.05 30.77% l 7 J1.1 . .............4‘5.. I......... 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 52459 ■TMslOhe IL, 1 i, 1 5.5,5-bezamefi ,1 3 3-biat iner 73 147 I ■ ■ i ' ■ > ■ । ■ 281 32.80 33.00 33.20 33.40 5000 m/z 281.0.0 19.52%

369 207 249 338 1....................................... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacety!)-O,O’,O"-tris(trimethylsilyl)no TTar 73 32.80 33.00 33.20 33.40 355 m/z 355.05 19.38% 5000

45 | I, 120147 193 265 J 481 । ■■ ■ । ■ ■ 1 1 I ' 1 m/z~> 50 100 150 200 250 300 350 400 450 500 550 32.80 33.00 33.20 33.40

30707.D GCMS1126.M Mon Jan 28 11:24:38 2002 Page 13

NYC-WTC_000004455