GC/MS calibration data for sample 30643, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 33.08 2.79 ug/1 1250090 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 20 4 Benzoic acid. 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 11 Abundance Scan 3054 (33.080 mln): 30643.D (-) m/ z 73.0.0 100.00% 73

147 5000 221 355 281 . , । . . . . । 1 .T| 1 I I l | 1 i 429 32.80 33.00 33.20 33.40

mlz-> 45 113. r “I t *r 1*" rfi . 50 100 150 +1911 +21— 200 250 , 325, , 401 t h , 1 P* t rirei h । . ■ TI J I I J l ' I 1 300 350 400 450 500 550 m/z 147.00 60.02% Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 1** 1* * ' Tfl l > l | > I 147 32.80 33.00 33.20 33.40 221 281 m/z 221.0 29.28% 327 415 519 561 1 ; • i • 1 • ' i • ■ • ■ i '• i ' ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 • • | • 1 J-fT'l 14144 281 32.80 33.00 33.20 33.40 5000 m/z 355.0 25.53% 369 207 249, 338 1 48,248*818***I***11*41W+S414*I*114*1414411*1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 32.80 33.00 33.20 33.40 m/z 281.0 20.89% 147 5000 267 355 429 45 207

TTI3 1 t I I 4 I I l r < > I I i f » I f l < I 4 { > I J ‘ ‘ • I ‘ ‘ *(**»» I * * * * 1 * 1 rrTtr TTTii PTT m/z-> 50 100 150 200 250 300 350 400 450 500 550 32.80 33.00 33.20 33.40

30643.D GCMS1126.M Fri Feb 01 10:48:41 2002 Page 14

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