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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 34.37 2.01 ug/1 901127 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 38 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 N-Benzhydrylidene- (2,4,6-trimethy 343 C24H25NO 089839-57-6 27 Abundance Scan 3195 (34.374 min): 30643.D (-) m/z 73.Q0 100.00% 73

147 5000 221 281 355 401 429 34.00 34.20 34.40 34.60 34.80 1 I"I 1 1 ■r">-f r’1 Ft —1914—2514 443271 19m 45 96 117.. m/z 147.00 50.22% m/z-> 50 100 150 200 400 250 300 350 450 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 ri ' 1 i 1 1 i ■ • ■ • i • 281 34.00 34.20 34.40 34.60 34.80 45 369 m/z 221.05 29.14% — 117 _ 297, 249, ......... |.............. m/z-> Abundance

5000 50 73 100 150 200 250 300 350 400 #538/1: 1-Monolinoleoylglycerol trimethylsilyl ether

147 207 450

A 1 • i • • ■ ■ i • 34.00 34.20 34.40 34.60 34.80 m/z 281.00 17.04% 34 103 281 395 482 » t______________ |_________________ !_______________________ |

» । » i i i S i i i । i i i ■ । » i r » । 11_____________I__________ 482 i > । ■ i i i । i i i i । i < > i ] i t i i i i miz-> 50 100 150 200 250 300 350 400 450 Abundance #71006: Ethanedioic add. bis(trimethylsily!) ester -rrm-vr■ mj" i r i '| i- 73 34.00 34.20 34.40 34.60 34.80 m/z 355.05 15.61% 147 5000

45 117 .. , , 190 219 ■ । . i i i । i i r i [11 . । 1 ‘ i ■ m/z—> 50 100 150 ' ' 260 ' ' 250 300 350 460' ‘ ‘ 450 ‘ 34.00 34.20 34.40 34.60 34.80

30643.D GCMS1126.M Fri Feb 01 10:48:45 2002 Page 15

NYC-WTC_000018465

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NYC-WTC_000018465Source: NYC Law Department, mirrored locally

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