NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30643.D Vial: 59
Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209
Mise Multiplr; 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
34.37 2.01 ug/1 901127 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5 -hexamethyl 384 C12H3604Si5 003555-47-3 38
2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38
3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32
4 N-Benzhydrylidene- (2,4,6-trimethy 343 C24H25NO 089839-57-6 27
Abundance Scan 3195 (34.374 min): 30643.D (-) m/z 73.Q0 100.00%
73
147
5000
221
281 355
401 429 34.00 34.20 34.40 34.60 34.80
1 I"I 1 1 ■r">-f r’1 Ft —1914—2514 443271 19m
45 96 117..
m/z 147.00 50.22%
m/z-> 50 100 150 200 400
250 300 350 450
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73
147
5000 ri ' 1 i 1 1 i ■ • ■ • i •
281 34.00 34.20 34.40 34.60 34.80
45 369 m/z 221.05 29.14%
— 117 _ 297, 249, ......... |..............
m/z->
Abundance
5000
50
73
100 150 200 250 300 350 400
#538/1: 1-Monolinoleoylglycerol trimethylsilyl ether
147
207
450
A 1 • i • • ■ ■ i •
34.00 34.20 34.40 34.60 34.80
m/z 281.00 17.04%
34 103
281 395 482
»
t______________ |_________________ !_______________________ |
» । » i i i S i i i । i i i ■ । » i r » ।
11_____________I__________ 482
i > । ■ i i i । i i i i । i < > i ] i t i i
i i
miz-> 50 100 150 200 250 300 350 400 450
Abundance #71006: Ethanedioic add. bis(trimethylsily!) ester -rrm-vr■ mj" i r i '| i-
73 34.00 34.20 34.40 34.60 34.80
m/z 355.05 15.61%
147
5000
45
117 .. , , 190 219 ■ । . i i i । i i r i [11 . ।
1 ‘ i ■
m/z—> 50 100 150 ' ' 260 ' ' 250 300 350 460' ‘ ‘ 450 ‘ 34.00 34.20 34.40 34.60 34.80
30643.D GCMS1126.M Fri Feb 01 10:48:45 2002 Page 15
NYC-WTC_000018465
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