GC/MS calibration data for sample 30643, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Ethanedioic acid, bis(trimethy Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

35.57 2.10 ug/1 622555 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 2 Trisiloxane, 1,1,1,5, 5, 5-hexamethyl 384 C12H3604Si5 003555-47-3 32 3 3-Isopropoxy-1,1,1,7, 6z7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 Butanoic acid. 3-me iyl-2-[ (trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 3325 (35.568 mln): 30643.D (-) m/z 73.00 100.00% 73

5000 147 221 i-1 r i /■ IM r 281 355 -r-pr-T 35.20 35.40 35.60 35.80 • • 1 ■

miz-> 45 117 0- ■ ’‘f"1 r ** । ■ TPr 50 100 150 +1914— 2514+,4.3271, 200 250 300 350 401 429 ■■r■i■ ■ ■ ■ i11111'1 400 450 500 550 m/z 147.00 49.69% Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73 147 110. . . । । > 5000 35.20 35.40 35.60 35.80 45 m/z 221.05 30.55%

miz-> 1. i 117 7 I »»i i । i i r r i' 190219....... .............................. 200 ' 250 300 350 400 450 500 ‘ 550 ' 50 100 150 Abundance #74103; Trisiloxane, 1,1.1,5.5,5-hexamethyl-3,3-bis[(trifnet 73 147 j Te * 21- 35.20 35.40 35.60 35.80 5000 m/z 281.00 18.29% 281 45 369 i . i 117 207 249 T » | i » »I | I I « » j I ill । < i i i । TT I-J । । i । । > ? । । । t ( । । । । । । । । n i 1 PT miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim -rm , 35.20 35.40 35.60 35.80 e m/z 355.0 13.47% 5000 147 221 281 327 415 t 519 561 » । | i > i t । i I i I । i * I IT’f I • | » i i | I i J i । I II I J I'T JTTf m/z—> 50 100 150 200 250 300 350 400 450 500 550 35.20 35.40 35.60 35.80

30643.D GCMS1126.M Fri Feb 01 10:48:50 2002 Page 16

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