Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
NYC-WTC_000033765–000033779Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28159.D Vial: 21 Acq On : 27 Nov 2001 6:15 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethanedioic acid, bis(trimethy Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 38.03 1.16 ug/1 204160 Perylene-dl2 37.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 35 2 Trisiloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5i 003555-47-3 25 3 1,2-Bis (trimethylsiloxy) ethane 206 C8H2202Si2 007381-30-8 16 4 Cyclopropan line, N-methyl-l-phenyl 147 C10H13N 056771-48-3 12 Abundance / Scan 3593 (38.032 min): 28159.D (-) m/z; 72.95 100.00% 73 .................... ........... 147
5000 221 281 355 TTTTTTTTTTPI , .. 429 37.80 38.00 38.20 38.40 43 191 TITpo4 TTTTTTTTHTTTTT 1 .... । fta m.t T T 327 L 401TTT mm T T m/z 147.00 73.92% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73
147 5000 37.80 38.00 38.20 38.40 45 m/z 221.05 46.54% ................. / | | 117.. . ................................ TTTTT TCTUu—gTTTTTT TT , T TCTICTETEITTETTT m-|-n i TITT"TTTEITTTT‘TT‘ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 TETEETIT _ 37.80 38.00 38.20 38.40 5000 m/z 207.00 30.76% 281 45 369 I , 117 207 249 . , HH| |, L p I 11 | H I 11 H H | I TT—TTTTTTTTTTT’ TTTTTTTTTTTTTTTTTTT T TT TTTTTTTTTTTTTT miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #70005:1,2-Bis(trimethylsiloxy)ethane 147 37.80 38.00 38.20 38.40 m/z 281.00 26.79% 73 5000
103 191 47 47 ,| , 1 .,i | TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT Trrrrj-r 1 I I m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 37.80 38.00 38.20 38.40
28159.D GCMS1126.M Wed NOV 28 11:15:54 2001 Page 3
NYC-WTC_000033774
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NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder