GC/MS calibration data for sample 30643, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Ethanedioic acid, bis(trimethy Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T.

38.01 0.75 ug/1 221447 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 35 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 3 3-Isopropoxy-1,1,1,7, 7, 7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Indapamide/ 365 C16H16C1N3O3S 026807-65-8 23 Abundance Scan 3591 (38.010 min): 30643.D (-) m/z 73.0.0 100.00% 73

147 5000 221 281

+191+ +234+,41327%. 40142...... 355 37.60 37.80 38.00 38.20 38.40 mlz-> 43 TTTr 50 117 1TPr . 100 150 200 250 300 350 400 450 500 550 m/z 146.9 57.94% Abundance #71006: Ethanedioic acid; bis(trimethylsily!) ester 73

147 5000 *TP109TTTRPrrr 37.60 37.80 38.00 38.20 38.40 45 m/z 221.0 34.27% 1._ L 117 1 ■ i ■ ■ ■ ■ i ' ‘ 190 219 ..... ........ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103; Trisiloxane, 1,1,1.5,5,5-hexamethyl-3,3-bis[(trimet 73 147 37.80 37.80 38.(X) 38.20 38.40 5000 281 45 369 ,117 1 207 2491 1*1*1***I*+-I***I* ’+*’’I’’ iz-> 50 100 150 200 250 3(X) 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7>717-hexamethyl-3,5,5-tris(trfm 73 37.60 37.80 38.00 38.20 38.40 m/z 281.00 18.70% 5000 147 221 281 327, 415 519 561 ms • ■ i ■ ■ ■ 1 i • 1 ■ ' i ■ • • ' i 1 f ■ ■ i ■ 1 1 ' i ' 50 100 150 200 250 300 350 400 450 500 550 i ■ ■ • ■ i ■ ■ • • i ■ ■ 1 ■ i ■ ■ ■ ■ i ■ 1 37.60 37.80 38.00 38.20 38.40

30643.D GCMS1126.M Fri Feb 01 10:48:59 2002 Page 18

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