Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Ethanedioic acid, bis(trimethy Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
35.57 1.52 ug/1 421995 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 35 2 Trisiloxane, , 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 Propanedioic acid, methyl-, bis (tri 262 C10H22O4Si2 040333-07-1 25 4 1,2-Bis(trimethylsiloxy)ethane 206 C8H2202Si2 007381-30-8 25 Abundance 73 Scan 3325 (35.571 min): 30708.D (-) m/z 73.00 100.00%
147 5000 185 221 55 355 281 ■ ’i ■ ' ■ ■ i 1 112
m/z-> 44 494+4 6,429 .240 m TTpT 325 | | 166 TI—mg 401 429 40 60. 80 1001201401601802002202402602803 00320340360380400420 35.20 35.40 35.60 35.80 36.00 m/z 147.00 54.33% Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester 73
147 5000 35.20 35.40 35.60 35.80 36.00 45 m/z 221.05 31.74% 117 190 219 m/z->___ 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 ' Abundance 874103: Tasilo and 1.1,1,5.5,5-hexamethy-3.3-bis(trimet 73 147 ' I ■ ' ' 1 1 1 1 ‘ ‘ I ' ' I 1 ' I 1 I 35.20 35.40 35.60 35.80 36.00 5000 m/z 185.10 30.11% 281 45 369 117 207 249 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #71770: Propanedioic acid, methyl-, bis(trimethylsilyl) est i I I > r r < | IT 147 35.20 35.40 35.60 35.80 36.00 m/z 57.00 2 0.98% 73 5000
m/z-> 445 | I 218 247 ....................... .............. I ■....... . ।।, T I........ I ................................................................ ।, ‘111 111111111111111111 n 111 > n r 11111! 11 > 111111! 1111111 u 11 40 60 80 100120140160180200220240260280300320 340 360380400420 MA MMM , , T ,Y, 35.20 35.40 35.60 35.80 36.00
30708 .D GCMS1126.M Mon Jan 28 11:29:22 2002 Page 15
NYC-WTC_000004354
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
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