NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV0201\24474.D Vial: 14
Acq On : 3 Nov 2001 3:41 am Operator: 209 GALOS
Sample ; gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Ethanedioic acid, bis(trimethy Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
39.63 0.50 ug/1 87078 Perylene-dl2 37.16
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanedioic bis (trimethylsily 234 C8H18O4Si2 018294-04-7 35
2 3,7-Dioxa-^8-disilanonane, 2,2,8,8 220 C9H24O2Si2 017887-80-8 35
3 Mercaptoaoetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 32
4 Pentanoiy acid, 2-[(trimethylsilyl) 262 CllH26O3Si2 055887-46-2 25
^bunclance Scan 3767 (39.629 min): 24474.D (-) m/z 73.00 100.00%
4*3
147
5000
221
281 355
44 177 253 39.20 39.40 39.60 39.80 40.00
96 117
'I‘ "I""I " I" " I" " I " Mt m/z 147.00 76.75%
■nfe-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #71005: Elhanedioic acid, bis(trimethylsilyl) ester
73
............... :.......................
147
22
39.20 39.40 39.60 39.80 40.00
45 m/z 220.95 49771%
117 . W 219
ML
T-ryn pn-rYyTMrpn-r^pTTTyrTTTjTTTnyrTTTpnT-TpTTTyTTTTpTTTy^^
TTfe-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #70531:3,7-Dioxa-2,8-disilanonane, 2,2.8,8-tetramethyl-
147
39.20 39.40 39.60 39,80 40.00
500) m/z 280.95 26.07%
73
115
■n/z->
Abundance
11 Lx 177 205
"' I" " r
40 60 80 100120140160180200220240260280300320340360380400420
#30949: Mercaptoacetic acid, bis(trimethylsilyl)-
1 ‘' I A
73 39.20 39.40 39.60 39.80 40.00
147
m/z 355.05 24.30%
5000
221
45
.1,,,
I " '' I' ’
104
■ 11" 'I"" I'"" I 1„,,.................... ........
Ti^-> 40 60 80 1OT120140160180 200 220 240 260 280 300 320 340 360 380 400 420 39.20 39.40 39.60 39.80 40.00
24474.D NP103001.M Tue Nov 13 10:08:09 2001 Page 4
NYC-WTC_000068471
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