NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C;\HPCHEM\1\DATA\NOV0201\24474 .D Vial: 14
Acq On ; 3 Nov 2001 3:41 am Operator: 209 GALOS
Sample ; gc/ms unknown Inst : GC/MS 209
Mise Multiplr; 1.00
MS Integration Params; LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library ; C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
41.58 0.63 ug/1 109514 Perylene-dl2 37.16
it# of 5 tative ID MW MolForm CAS# Qual
1 3,6-Diox^2,4,5,7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 40
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 27
3 Mercajfroacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 23
4 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 17
Abundance Scan 3980 (41.584 min): 24474. D (-) m/z 73.00 100.00%
73
147
221
5000
281 355
41 429 4120 41.40 41.60 41.80 42.00
, 96I 1 I 119, 191
1^31 I I [ I iVi I m/z 146.95 74.33%
TTfe-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7-
147 z;i
73
HilWi
41.20 41.40 41.60 41.80 42.00
191 m/z 220.95i57.91%
117 279
I ‘' I I'"' i'"' I" ‘' I r "' 1" " I'' ‘' I'''' I
Tl/Z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester
73
147 41.20 41.40 41.60 41.80 42.00
5000 m/z 207.00 37788%
45
I. I .......-'.17........ 219
nZz-> 40 60 80 100120140160180200220240260280300320340360380400420
^bundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)-
73 41 20 41.40 41.60 41.80 42.00
147
m/z 281.00 26.07%
5000
221
45
I 193
104 _________ 1 L
TTTttt+tt +t i" " l‘ ‘ " I" " I " " I " " I" " I ” "I "'' I
nfe-> 40 60 80 100120140160180200220240260280300 320 340 360 380 400 420 41.20 41.40 41.60 41.80 42.00
24474.D NP103001.M Tue Nov 13 10:08:11 2001 Page 5
NYC-WTC_000068472
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