NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\SEP2801\22652.D vial: 11
Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DAT7kBASE\NBS75K.L
*********************************************************************
Peak Number 16 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
38.18 0.47 ug/1 67537 Perylene-dl2 37.29
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxax2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 23
2 2,6-Dim^hyl-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 16
3 MercajJtoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 12
4 B^rr^ophenone-2,4 ' , 5-tricarboxylic a 356 C19H16O7 000000-00-0 12
Abundance Scan 3610 (38.179 min): 22652.D (-) m/^ 73.00 100.00%
73
147
221
5000
281 355
429 JZ80_ja00_J8J0_3a40_38^
rrfe->
A I 1^ 193||
40 60 80 100120140160180200220240260280300320340360380400420
249 I
Mr _JL
I"" I"" I m/z 147.00 70?^
Abundance #41682: 3,6-Dioxa-2,4,5.7-tetrasilaoctane, 2.2,4,4,5,5,7,7-
147 Zil
73
5000
37.80 38.00 38.20 38.40 38.60
191 m/z 221.0061.16%
117 279
I I
I" " 1'''' I I'"' I
L
tVz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #44359:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridi
73 2|1
_J7^g_3a00_3820_3a40_38^
5000 147 m/z 207.00 32.24%
178
45
I, 296
ll......... I.. I""l
40 60 80 100120140160180200220240 260280300320340360380400420
^bundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)*
73 37.80 38.00 38.20 38.40 38.60
147 m/z 281.00 29.95%
5000
221
45
nZz->
Xv
1 ’I I 104
Tf+rr I ‘ '"I 11" " I" " I" " I •' " I" " I" "I
40 60 80 100120140160180 200 220 240 260 280 300 320340 360 380 400 420
I'"'!
37.80 38.00 38.20 38.40 38.60
22652.D NP091101.M Wed Oct 03 11:53:35 2001 Page 16
NYC-WTC_00b087296
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