Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
NYC-WTC_000088905–000088934Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search ’Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
39.74 3.02 ug/1 288392 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3 ,'6-Dioxa-2,4/^5,7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 33 2 1,2-Benzene^carboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 27 3 2,6-Dimeth/1-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 17 4 Mercaptoa^zfetic acid, bis (trimethyls 23 6 C8H2 0O2SSi2 006398-62-5 12 Abundance Scan 3779 (39.737 min): 23503.D (-) m/z 73.00 100.00% 7^
JI 147 221 5000 281 355 . T T 401 429 39.40 39.60 39.80 40.00 41 96 117 . r. I.1111.. .■ I..( m/z 147.00 72741%
1; TiZz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5.5,7,7- 147 2:;i
73 5000 __M40_ja60_39;80_40n0__ 191 m/z 221.05 53.98% 117 279 I " " P " 'b " ' I' “ ' I " " I " " I " n I'' " I " " I I TiZz-> 40 60 80 100120140160180200220 240260280300320340360380400420 ^bundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e _____________________ ,1|7__ ._ T 73 39.40 39.60 39.80 40.00 5000 m/z 281.00 77787%
45 295 119 . ' • I ” " I" Tife-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #44359:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridi
. ~ ,/v -73 2;i 39.40 39.60 39.80 40.00 -m/z. 354.95- 22-.-24%
5000 147 178 45 I I I 296 "I "I“ r. I I I ■ I I i < I r I I f .■
Ti/z-> 40 60 80 100120140160180200220240260280300320340360380400420 39.40 39.60 39.80 40.00
23503.D NP091101.M Thu Oct 18 10:29:17 2001 Page 17
NYC-WTC_000088928
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NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088207
Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088263
Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088853
Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088556
Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088372
Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089476
Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088316
Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
Filed in the same folder
NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
Filed in the same folder
NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
Filed in the same folder
NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
Filed in the same folder