NYC 9/11 Public Portal Document
Library Search Compound Report
Data File ; C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11
Acq On : 17 Oct 2001 12:01 am Operator: 2 09 GALOS.
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 16 Tris(trimethylsilyl)borate Concentration Rank 12 .
R.T. EstConc Area Relative to ISTD R.T.
38.14 1.38 ug/1 131893 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Tris(trimethylsilyl)borate 278 C9H27BO3Si3 004325-85-3 27
2 1-Monoli/foleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25
3 3-IsopXopoxy-l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 16.
4 Merc. toacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 12
Abundance ' Scan 3605 (38.139 min); 23503. D (-) m/ z 73.00 100.00%
73
147
5000 221
281 355
, 1?3i 429 37.80 38.00 38.20 38.40
44 233,1 1 325.
............................ m/z 147.0062741%
Tl/Z-> 50 100 150 200 250 300 350 400 450 500 550
'\bundance #39028: Tris(trimethylsilyl)borate
73 221
5000
37.80 38.00 38.20 38.40
263
m/z 221.05 47.20%
133 175
.......... .......... .J .I , ,l. « t, ,1, , ,1..............................................................
nZz->_______ 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
-73- -
207
37.80 38.00 38.20 38.40
5000 147 m/z 281.00 22^11%
34 103
281
1 J_l
395
-I- . 482
Ti^-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris{trim
73 .- 37.80 38.00 38.20 38.40
m/z --35 5=^0 5 20.20%
5000
147
Tl/Z-> 50 100 150 200 250 300 350 400 450 500 550 37.80 38.00 38.20 38.40
23503.D NP091101.M Thu Oct 18 10:29:15 2001 Page 16
NYC-WTC_000088927
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