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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088926
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Tricosane Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 36.37 1.09 ug/l 103733 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 90 2 Pentacosane 352 C25H52 000629-99-2 90“ 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 86 4 Pentadecane_________________________ 212 C15H32 000629-62-9 86 Abundance Scan 3412 (36.368 min): 23503.D (-) m/z 56795 100.00% 57 71 43

5000 85

99 4 40 36 00 36.20 36.40 36.60 207 281 I''' ' I'' '' I' ''' I ■raTz 71.00 83.31% Ti/i-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318; Tricosane 3 57

71 5000 85 ‘.“fC*. Cl I . . { . I ?7'i“, " . 1 lA 36.00 36.20 36.40 36.60 m/z 43.00 67.46% I ?T;?714i 183197211225 296 324 I ' • * 'I ' ' ' ' I I I i I I • ' I ' ' ' I ' ' ' ' I ' ' ' I' ''' I ‘' I '' I ‘' 11' 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73718: Pentacosane 43-5,7 ........... ' ' ' ' I ' ‘ ‘ ' I ' ' ' ' I ' 71 36 00 36.20 36.40 36.60 5000 m/z 85.05 48.60% 85

1P127141155169183197211225 T^yTTTh-pVrT-jh-TTryTrTTq-rT-TT-JTTT-T^^ nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- -tAA 7..^ 36.00 36.20 -36.40 36.60-- 71 m/z 55 .-00-“ 28.04%

5000 85

T 183 211 268 296 '' I '' I ' ‘' I' TTT^Y'rT^^"rp4rT-rfTTTYyTT-rTjVT-TTprTtT-p-m-^^ Tl/Z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ' 36.00 36.20 36.40 36.60

23503.D NP091101.M Thu Oct 18 10:29:13 2001 Page 15

NYC-WTC_000088926

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NYC-WTC_000088926Source: NYC Law Department, mirrored locally

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