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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088222
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tricosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.70 2.22 ug/1 244003 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tricosane 324 C23H48 0O0638-67-5 91. 2 Heptadecane 240 C17H36 000629-78-7 91 / 3 Heneicosane 296 C21H44 000629-94-7 90 / 4 Octadecane 254 C18H38 000593-45-3 90 ' \bundance Scan 2796 (30.705 min); 23320.D (-) m/z 57.00 100.00% 57

43 71 85 5000 _____ n_____ Ui -I I I 1 1 1 I I 1'1 I , I I I I ■ I 1 1 I 99 30.40 30.60 30.80 31.00 1 J 155169183197211 267 324 239 ' I''' ' I'' ' I' '' m/z 71.00 67.95% TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318; Tricosane 3 5(7

71 5000 85 30.40 30.60 30.80 31.00 m/z 43.05 62.83% j J y113127141 183197211225 296 324 1 ' ' ' U "' ' ' I ' ' ' ' 1 '' ' ' I ' p-rTTy^rTTT*yTT-r-q-rTrT I' '''I ' ' I ' ' ' ' I I ' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193; Heptadecane 57 1 T 71 30.40 30.60 30,80 31.00 5000 m/z 85.05 50.45% 85

99 J J 155169 210 240 11' 11111 ' I ' ' I ' I ' ' ' ' I' ' ' ' ' I ' ' I I''' ' I'' " I' ' r ''' I •''' I'' ’ H ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 57 30.40 30.60 30.80 31.00 71 m/z41.00 25.13% 85 5000

99 268 296 I I . . . I 1 » V » J .\ , J 1 . . 1 J I *''' r ' ' ' r ' ' ' I p-TTTYTTTt-l- •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

23320.D NP091101.M Mon Oct 15 09:53:50 2001 Page 9

NYC-WTC_000088222

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NYC-WTC_000088222Source: NYC Law Department, mirrored locally

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