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GC/MS analysis results for sample AD23345, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.

NYC-WTC_000088556–000088584

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088571
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23345.D Vial: 17 Acq On : 10 Oct 2001 4:57 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 9 Tricosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 30.70 3.39 ug/1 297021 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 94 2 Heneicosane 296 C21H44 000629-94-7 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Docosane, 9-butyl- 366 C26H54 055282-14-9 91 Abundance Scan 2795 (30.702 min): 23345.D (-) m/z SYTOO 100.00% 57

43 71

5000 85

99 I''' I 30.40 30.60 30.80 31.00 I. .J j J 225 253 324 -|-r-T-i m/z 71.00 70.59% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 413 57

5000 71 85 .... JV... . 30.40 30.60 30.80 31.00 m/z 43.05 66.19% Ik 113127141 183197211225 296 324 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane

553 57 71 85 1 30.40 30,60 30J0 31.00 m/z 85.05 47.41% A 99 268 296 '' I' I'''' I'''' I'''' I pm-rp-n-t-p Ti/z-> Abundance 40

43 60 80 100 120 140 160 180 200 220 240 260 280 300 320 #72323: Eicosane JL T' ' ' M 30.40 30.60 30.80 31.00 m/z 41.00 28.68% 71 5000 85

n/z-> 40 ■rpn“ 60 80 113127141 ‘ I ’ ’ ' ' I ' ' I'' ' ' ' I ' ' ‘ ' I 100 120 140 160 180 200 220 240 260 280 300 320 pr-m-p-r-n-y 282 ' I' ' ' ' I'' '' I .JI..... 30.40 30.60 30.80 31.00

23345.D NP091101.M Thu Oct 11 13:10:17 2001 Page 9

NYC-WTC_000088571

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NYC-WTC_000088571Source: NYC Law Department, mirrored locally

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