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GC/MS analysis results for sample AD23319, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088444
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT12 O1\23319.D vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tricosane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 30.70 1.96 ug/1 204794 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Tricosane 324 C23H48 000638-67-5 95 2 Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 2795 (30.702 min): 23319. D (-) Wz 57.00 100.00% 57 A 43 71

5000 85

30.40 30.60 30.80 31.00 pVrrf-rT-rVpn'-TT-YTTn-rYT-rTTq-T-i-r-rpn-Tn-p-rTn-yT-^^ m/z 71710 79735% v/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 5 7

71 / V 5000 85 I ' ' 30.40 30.60 30.80 31.00 m/z 47705 74724% , 99

■Ti/z-> '' I' 40 60 LA 80 113127141 183197211225 296 324 I I ■ I I I ■ n-q I I.< I I I I i I ■ I I <I Ii I I I< I I , I ■ >I ■ I

100 120 140 160 180 200 220 240 260 280 300 320 rr-rp-T-TTy-t-n

Abundance #39862: Eicosane 43 57 I rf 71 30.40 30.60 30.80 31.00 702 85 m/z 85.05 46733%

I , 7 113127141155 196 240 ^82 Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 1 5|7 30.40 30.60 30.80 31.00 43 71 m/z 41.05 27705%

522 85 ft 99 JI. |i| 224 254 I ' ' ' ' I ryT-r-rTyrrVrp-rT-rp-rTT-p-rT^ ■n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

23319.D NP091101.M Mon Oct 15 09:49:39 2001 Page 9

NYC-\/VTC_000088444

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NYC-WTC_000088444Source: NYC Law Department, mirrored locally

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