GCMS analysis results for sample AD28471, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\DECO4O1\28471.D vial: 7 Acq On 4 Dec 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Tit ie : 209 625/TCLP calibration table Library : C:\DATABASE\NBS 7 5 K.L ********************************************************************* Peak Number 4 Tricosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.63 0.89 ug/1 232880 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qu.

1 Tricosane 324 C23H48 000638-67-5 97 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 2787 (30.632 min): 28471 .D (-) m/z 57.00 100.00% 43 57 71 85 500U —................ ... ।

99 113 30.40 30.60 30.80 31.00 J|J |,I , 137141155169183197211225239 "Hrim ; "Tmmm f 324 m/z43.05 75.00% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundan. #73318: Tricosane 43 57 I 71 5000 85 5T i T m T 1 T 30.40 30.60 30.80 31.00 m/z71.10 66.19% 22 113127141 183197211225 296 324 | - -p-m rm-rj-m TT’I TTTItur ' ' I ' ’ I'1111 miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 43 71 30'40 30.60 30.80 3t00 85 5000 m/z 85.05 51.00% 99 ! 4 .................... . HT miz->40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32063: Heptadecane ----- T 57 30.40 30.60 30.80 31.00 i 71 m/z 41.05 29.59% 85 5000

99 113 17141 196 240 — MTTM f i TTP 4 4 TT ■ ■ i " ■ ■ i ■■ ■ ■ i ■ ■ ’ ■ r"' ■ i •■ ■ ■ i ■ "TTT’TTT TT"I0"‘I1111 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

28471.D GCMS1126.M Wed Dec 05 11:27:36 2001 Page 4

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