GCMS analysis results for sample AD28471, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD28471 conducted on December 6, 2001.

NYC-WTC_000034347–000034365

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28471.D Vials 7 Acq On 4 Dec 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Tit le : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K . L ***************************************************** * * * * * *********** Peak Lumber 5 Octadecanoic acid, 2-methylpro Concentration Rank 2 R. EstConc Area Relative to ISTD R.T. 31.57 4.56 ug/1 1198560 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecanoic acid, 2-methylpropyl e 340 C22H44021 000646-13-9 87 2 Butyl tetradecanoate (myristate) 284 C18H36021 000000-00-0 64 3 Octadecanoic acia, butyl ester 340 C22H4402 000123-95-5 33 4 1- • I exene, 2-methyl- 98 C7H14 006094-02-6 27 Abundance Scan 2889 (31.568 min): 28471.D () m/z 56.00 100.00% 56

5000 41 I 73 129 285

mlz-> 4lll,211,143 171185213 241 27 311 340 m/z 57.00 ‘i 40 60 TTTTTTITTTIT i "■■ i■ ■11 r11 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31 20 31,40 31,60 31.80 56.38% Abundance #48214 Octadecanoic acid, 2-methylpropyi ester 57

) 5000 TT I ■ ' r • I T 1" 3120 31.40 31.60 31.80 285 m/z 43.05 46.78%

m/z-> 73 ‘TITT i ■ ■ ■ ■ i' 40 60 80 mA . 97 114 129 185 241 i ■ ■ ■ ■ i ■ ■ ■ ■ I'' " I " " i " " I'' 100 120 140 160 180 200 220 240 260 280 300 320 340 7— 340 111 " " I " 1 Abundance #40186: Butyl tetradecanoate (myristate) 56

3120 31.40 31,60 31.80 500C m/z 41.05 41.94% 229 73 211 129 284 i. 185 | -101 I m... HP - mz->. _ 40 Abundance 60

56 80 100 120 !40 160 180 200 220 240 260 280 300 320 340 #73570: Octadecanoic acid, butyl ester ...... IW... 1 p 1 ' • I ' ' ' ’ I ' ' 1 1 I 1 1 ' ' 1 ’ 31.20 31.40 31.60 31.80 m/z 55.00 31.61% __ 5000 285 340 73 267 129 k 185 241

m/z—> 40 L4427111 60 __________ L___________ i ■ ।.... ।.... । j .., ।. 11.11111 p । 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘ I " I •" ’ I ’' 1 1 1 31.20 31,40 31,60 31.80

28471.D GCMS1126.M Wed Dec 05 11:27:38 2001 Page 5

NYC-WTC_000034358

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NYC-WTC_000034971

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