Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
NYC-WTC_000087496–000087516Folder label: “GC/MS Scan 9/20/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On : 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample : 9/20 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Octadecanoic acid, 2-methylpro Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.67 1.34 ug/1 204617 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual fl)Octadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 87 Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 86 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 56 4 Pentadecane, 8-methylene-224 C16H32 055668-09-2 32 Abundance Scan 2901 (31.669 min): LB.D (-) Wz 56.00 100.00% 55
5000 4’ 73 I 29 285 ...... ............ JL .1 lU.Jh Al ,153 171^85^99 340 227241 | 31,40 31,60 31,80 32,00 I I p‘ I 1"T^ ( f rrtn 11 I I i'tT |"f I I I I I I i I I I I \ 11 I > I I *1 I u I I 11 I I i'tti ■! I 11 I I j rm'| m/z 57.00 52770% nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5|7
253 rOi I n 31,40 31,60 31,80 32,00 285 267 m/z 43705 43.96%
■n/z-> 40 60 XuUuX ' ' ' I ' ' ' ' I ' ' > rj " ” J 185 241 I " " 1 •' " I' " ' I' " ' I'' " I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 [ 340 ft ^bundance #40186: Butyl tetradecanoate (myristate) 55 T ,-1". r r. I , , , , I 1 I r. "I m- 31,40 31,60 31,80 32,00 5000 m/z 41.05 38.69% 229 73 211 129
'nlz~> 40 T-rp-r 60 80 ■...... T..., pn-TT7-rT-r-ryT‘-r-TTj-rT-YTy^ 100 120 140 160 180 200 220 240 260 280 300 320 340 I...... ...T. Abundance #73570; Octadecanoic acid, butyl ester 53 31,40 31.60 31,80 32,00 m/z 73.00 32.99%
250 285 340
■nfe-> 40 60 u 73 129 185 I I “ " I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 241 "I•"H 267
" I r. • I'" ’ I t 31,40 31,60 31,80 32,00
LB.D NP091101.M Wed Oct 03 10:10:00 2001 Page 8
NYC-WTC_000087509
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 2, 2001.
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