Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
NYC-WTC_000087496–000087516Folder label: “GC/MS Scan 9/20/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample 9/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Pentacosane Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 31.77 1.18 ug/1 179169 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Pentacosane 352 C25H52 000629-99-2 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Tetracosane 338 C24H50 000646-31-1 90 Wsundance Scan 2912 (31.770 min): LB.D (-) m/z 57.00 100.00% 57 71 43 85 5000
31 40 31.60 31.80 32.00 32.20 ' ' I ' m/z 71.10 71.86% TlZ2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73718: Pentacosane 4b 57
I I ' ' ' ' I /\r I |7Tl 1 I 1 I . . I 1 71 5000 85 31 40 31.60 31.80 32.00 32.20 m/z 43.00 64.84%
■n/z-> -n-p-r 40 uu 60 80 169 183 197 211 225 '1 ' ' ' ' I ' ' ' ' i’' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 I ' ' * ' I ‘ ‘ I
Abundance #42201: Heneicosane 57 71 85 31 40 31.60 31.80 32.00 32.20 5000 m/z 85.05 53.69% 99 J 268 296 iiyz-> '' I' 40 JU 60 80 100 120 140 160 180^200^^0 240 260 280 300 Abundance #71561: Octadecane 31 40 31.60 31.80 32.00 32.20 43 71 m/z 41.05 26.73% 85 5000
■n/z-> u 60 ■
80 99 ..................................................................
100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00 32.20
LB.D NP091101.M Wed Oct 03 10:10:02 2001 Page 9
NYC-WTC_000087510
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086981
Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088456
Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088346
Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.
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Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 2, 2001.
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