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GC/MS calibration data for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.

NYC-WTC_000087496–000087516

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On : 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample : 9/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.76 1.20 ug/1 183463 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolFoirm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 90 2 Tetracosane 338 C24H50 000646-31-1 90 3 Octadecane 254 C18H38 000593-45-3 90 4 Tricosane 324 C23H48 000638-67-5 8? Abundance Scan 3020 (32.762 min); LB.D (-) m/z 57700 100.00% 57

43 71

5000 85

32.40 32.60 32.80 33.00 , 1,1 37211225,239,, 281,,,,,,,,,,,,,,, m/z 71710 70.52% Tl/z-> Abundance 40 60 5|7 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #42201: Heneicosane A 71 85 5000 32.40 32.60 32.80 33.00 99 Wz 43.05 65.25% I I ll ............................ 268 296 ■nlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #73543: Tetracosane 43 57 71 JL 3Z40 3Z60 3Z80 33.00 5000- 85 m/z85.0546.11% A 99 ■•'>3127 ll I 155169183197 294 338 '' I' I ’ ‘ ' I ' ' ' ' I T-fT ' I ' ' ' ' I ' ' ' ' I " " I ' ' ' ' I " " I ' ' ' ' I ' ' " I ' ' " I ' ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #71560: Octadecane 43 5 7 32.40 32.60 32.80 33.00 m/z 41.05 26751% 71 5000 85

93 n-s 'I' ' I I''' ‘JI' ‘J ' I'''' I •''' I169183197 ' ' I '■'' ■' I' 254 ni/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

LB.D NP091101.M Wed Oct 03 10:10:04 2001 Page 10

NYC-WTC_000087511

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NYC-WTC_000087511Source: NYC Law Department, mirrored locally

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