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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087991
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT04 01\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 6 Heneicosane Concentration-Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.73 1.05 ug/1 180950 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91' 2 Tetracosane 338 C24H50 000646-31-1 91- 3 Docosane 310 C22H46 000629-97-0 87 4 Tricosane 324 C23H48 000638-67-5 87 /Abundance Scan 2798 (30.730 min): LB.D (-) m/z “57.0,0 ’10o’. 00% 57 43 71 85 5000

hi/z-> XI 40 , J, ,1, •*55169183197211 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00 m/z 71.0„0 69.66% Abundance #42201: Heneicosane 57

5000 85 I / y 30.40 30.60 30.80 31.00 99 m/z 43.05 69.06% 268 296 nrTT’Y^T-t-TYT'VT-T-|^^ I''' ’ I f-r-rTTjTT-rtp m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane -43 57 ' 71 T 30.40 30.60 30.80 31.00 5000 85 m/z 85.0,5 50 147% 99 IIS t d .= '’F 155169183197 294 338 ■n/z-> 40 60_ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72997: Docosane . ....... \. ...... 43 5,7 30.40 30.60 30.80 31.00 m/z 41.0.5 26.71% 71 5000 85

11 II 11 r 11.1 iT.. 1. 11.1. i 1-^ I«i'.. I 111 292 310 . I ■RI' ' I''' * I'''' r*"'"'' 1 ’ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

LB.D NP091101.M Tue Oct 09 12:51:25 2001 Page 6

NYC-WTC_000087991

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NYC-WTC_000087991Source: NYC Law Department, mirrored locally

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