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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087992
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise 'Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 5

R.T, EstConc Area Relative to ISTD R.T.

31.67 1.95 ug/1 336691 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

i Butyl tetr^ecanoate (myristate) 284 C18H36O2 000000-00-0 64 2 Octadeca: ic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 45 3 Octadec^ loic acid, butyl ester 340 C22H44O2 000123-95-5 45 4 CyclopXopane, 1-(1-methylethyl)-2-n 210 C15H30 _________ 041977-39-3 27 Abundance 4 Scan 2900 (31.666 min): LB.D (-) m/z 56.00 100^0%

5000 4 73 29 285 .................... 340 31.40 31.60 31.80 32.00 Ki I I T I «‘V| I • r r I T f I I I I I r i' I I p I I I I I J 'i I I f I I I I I I I I t t I I I I I « I f l I I I -d- m/z 57.00 53.46% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 5(6

5000-

211 229 .... ML..... m/z 31.40 31.60 31.80 32.00 42.69% 129 185 284 1 ?7 101 I, 1 i I I T' ‘ ' I -p-n ‘m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-!nctnylpropyl ester 57 I . ........ /,V,y.o...... I 31.40 31.60 31.80 32.00 5000 m/z 41.05 38.37% i 73 267 285 I A i I Hi t 185 241 ! 340 I '' ' ' I ' I ‘ ’ I ' * ' ' I '''' 1 ' ' ‘ ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48208: Octadecanoic acid, butyl ester 56 31.40 31.60 31.80 32.00 m/z 55.00 30.92% c 285 73

a 129 267 340 97185 241 I I _L __ I t ‘T'W- '' ‘ I'''' I I'' ‘' I' ''' I '''' I' ''' I ‘ I' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

LB.D NP091101.M Tue Oct 09 12:51:53 2001 Page 7

NYC-WTC_000087992

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NYC-WTC_000087992Source: NYC Law Department, mirrored locally

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