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GC/MS analysis results for sample AD23260, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23260 conducted on October 12, 2001.

NYC-WTC_000088079–000088097

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23260 .D Vial: 6 Acq On 9 Oct 2001 6:15 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butyl tetradecanoate (myristat Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 31.65 0.91 ug/1 174.776 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 0 Butyl tetradecanoate (myristate) 284 C18H36O2i 000000-00-0 80 2 Octadecanoic acid, butyl ester 340 C22H44O2: 000123-95-5 28 3 1-Hexene, 2,5-dimethyl- 112 C8H16 006975-92-4 27 4 Cyclobutane, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 25 Abundance Scan 2898 (31.645 min): 23260.D (-) m/z SP/OO 100.00% 5S

5000 4' 73 ^29 285 ...... /Ur.,..,... TiZz-> UuM 20 40 60 I'. ■'Hl ..,1,..... .'*57 ,.207 TryiVnyTTTT'p'TVrpTTT'yTTrTpVrT^pTTT-Y'rrTTqHTTT'TTTTTjTVrTy^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 241 267 | 340 rrrtrr m/z 31.40 31.60 31.80 32.00 57.00 49.36% Abundance #40186: Butyl tetradecanoate (myristate) 5^

5000 229 31.40 31.60 31.80 32.00

Ti/z-> Abundance 20 -p-n-rp-r 40 u 60 73 129 211

I ' ’' ' I '' ' ' I' ' ' ‘ I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73570: Octadecanoic acid, butyl ester 284 m/z 43705 45767%

5|5 i-TTTnT, f. , . 31.40 31,60 31.80 32.00 5000 m/z 41.05 37.55% 285 340 73 129 267 185 241 I I I'''' I'''' I' ‘' I'''' I'''' i'' ‘' i '' Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #2706:1-Hexene, 2,5-dimethyl- I ' ' ' ' r* ' ' ' I ' f Sb 31.40 31.60 31.80 32.00 m/z 55.00 30767%

5000

27 112 I I ,1, 84 pTTlrp-r-rT-p-rTTp-rTTp-rrT-p-TT^ I' ''' I ''' ' I •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23260.D NP091101.M Thu Oct 11 10:43:56 2001 Page 4

NYC-WTC_000088089

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NYC-WTC_000088089Source: NYC Law Department, mirrored locally

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