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GC/MS analysis results for sample AD23081, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23081 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087842–000087862

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087853
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0 3 01\23081.D Vial: 8 Acq On 3 Oct 2001 7:29 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl tetradecanoate (myristat Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.67 1.09 ug/1 161685 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetrad^anoate (myristate) 284 C18H36O2 000000-00-0 72 2 Octadecanoi/f acid, butyl ester 340 C22H44O2 000123-95-5 64 3 Octadecan^c acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 46 4 1-Penter;e, 2,4-dimethyl- 98 C7H14 ___ ^02213-32^3 27 Abundance /....................... Scan2^3t670min): 236810(-)' m/z..... 56 . o’o.... iOO " 00% 53 A 5000 4 73 I 285 ................ ......................... , IJ 111 11 uF, , .'’.‘^2157171^^^199 227241 267 J 340 31.40 31.60 31.80 32.00 ... I" m/z 57.00, 50.35% m/z-> ,^J0__ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #40186: Butyl tetradecanoate (myristate) 5te

5000 229 31.40 31.60 31.80 32.00 , ? ^29 211 284 m/z 43.05 41.47% i I ?7l01 I I m/z--> 40 7TTn‘Tq-T-TTnYrTTTp-i‘T-^ 60 r‘ ' ' ' I • ' ' ' I ' ' ' ' I • ' ' ' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 4^ Abundance #73570: Octadecarioic acid, butyl ester 56

31.40 31.60 31.80 32.00 5000 285 m/z 41.0,5 36.32% 73 129 267 340 ft 185 I ' ' ' ' I ' ' ' ' I I i ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: bctadecanoic acid, 2-methylpropyl ester I 57 31.40 31.60 31.80 32.00 m/ Z 73.00 29.66% 5000 ft 285 267 j 185 241 I I 340 t •' ’' I' • ” I T ' I ' ' ' ■ I ' I • ' I r, . , I I '''' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23081.D NP091101.M Tue Oct 09 10:05:14 2001 Page 5

NYC-WTC_000087853

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NYC-WTC_000087853Source: NYC Law Department, mirrored locally

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