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GC/MS analysis results for sample AD22977, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22977 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087731–000087753

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22977 .D Vial: 3 Acq On 3 Oct 2001 2:36 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

31.67 0.45 ug/1 62099 Chrysene-dl2 33.16

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Butyl tet/adecanoate (myristate) 284 C18H36O2 000000-00-0 72 2 Octadecarioic acid, butyl ester 340 C22H44O2 000123-95-5 72 3 Octadec .oic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 49 4 1-Pent^ e, 2,4-dimethyl- 98 C7H14 002213-32-3 27 <\bundance Scan 2901 (31.670 min): 22977.D (-) m/z 56.00 100.00%

5000 4 73 I I 129 285 Vi V I L 1-| . - ,1 iM .gZiriy 1 143 1711B5 241 267 ] 31.40 31.60 31.80 32.00 1 I ' ' 11 [ I I I I |Ti ii I I I iT| I I O"| I I I I I I II I I II I I I II I I I I I I ' I I I I I I I I I r i'i“r| 340 m/z 57.00 51.70% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate)

5000 .......... . 229 31.40 31.60 31.80 32.00 , ? 129 211 m/z ^3.05 48.38% 284 i '' I' !l I I I I ' I ' ' ' ' I ' ' ^’ l ■ I l - I'''' I 4^ I " ' ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 56 . ...... MU-,... 31.40 31.60 31.80 32.00 5000 285 m/z 41.05 43.78% 340 73 129 267 185 241 : j ... I ''I'' I"' ' " I ' ' ' ' I ' ' I 11 ‘ ' 11'' " I " '' I " '' I' " ' I " '' I' " ' I " " I " " I'' " I " m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methyipropyl ester 5f7 31.40 31.60 31.80 32.00 m/z 73.00 33.49% 5000 285 267 J

'n/z-> 40 60 185 80 100 120 140 160 180 200 220 240 260 280 300 320 340 241 I I ' l'' ' ' ' I ' *' ' I ’' ' ' I T 340 ....... l\,(\..... 31.40 31.60 31.80 32.00

22977.D NP091101.M Tue Oct 09 09:48:38 2001 Page 7

NYC-WTC_000087744

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NYC-WTC_000087744Source: NYC Law Department, mirrored locally

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