GC/MS analysis results for sample AD23502, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23502 conducted on October 19, 2001.

NYC-WTC_000088880–000088904

Folder label: “GC/MS Scan 9/27/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1601\23502 .D Vial; 10 . Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.65 3.19 ug/1 375270 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl tetradecanoate (myristate) 284 C18H36O2 ,000000-00-0 64 2 Octadeca: ic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 62 3 Octadec^noic acid, butyl ester 340 C22H44O2 000123-95-5 47 4 Cycl^utane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance Scan 2898 (31.648 min): 23502.D (-) m/z 56.00 100.00% 53

253 4' 73 129 285 T JJJ I 143157171'*^ 213227241 340 31.40 31.60 31.80 32.00 . TTi-p I . 1 I I .'1 ' I i I . . I. I r I . . . r I r. . . J I iT. p . . . j . . . . । . i . i j r. . ■’■I'''" I"" t" m/z 57.00 50.83% tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186; Butyl tetradecanoate (myristate) 53

......... ............. 5000 229 31,40 31,60 31.80 32.00 211 m/z 4^705 41.59% 284 p-T-rrpHT-rpT-^-T-f-rt'rTp-T^^ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyi ester c: 7-

31.40 31.60 31.80 32.00 5000 m/z 41.05 38.00%

■n/z-> ^bundance 40 60

53 IaXuxX 111 pf i I 11 111 r I... 11 185 I'' ’' I''' ’ I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #48208: Octadecanoic acid, butyl ester 241 340

JL ----- - 31.40 - 31.60 31.80 - 32.00 - -m/z—73.00 30.27%

5000 285 -73 -- ---------- 129 267’ "340 185 241 I I I 111 ‘ • 11' 1'' I I'''' I'''' I'''' I'' '' I ' ' I ' ' ' ' I ' ' ’ I ' ' ' ' I ' ' 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260.280 300 320 340 31.40 31.60 31.80 32.00

23502.D NP091101.M Thu Oct 18 10:24:59 2001 Page 9

NYC-WTC_000088895

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