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GC/MS analysis results for sample AD22779, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22779 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087694–000087716

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087707
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\22779.D Vial: 16 Acq On : 3 Oct 2001 4:48 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.67 0.94 ug/1 137358 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual CvButyl tetradecanoate (myristate) 284 C18H36O2I 000000-00-0 80 2 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2; 000646-13-9 60 3 Octadecanoic acid, butyl ester 340 C22H44O2: 000123-95-5 56 4 1-Pentene, 2,4-dimethyl- 98 C7H14 002213-32-3 27 /Kbundance Scan 2900 (31.667 min): 22779.D (-) m/z 56.00 100.00% 55 ft 5000- 4' 73 285 lA * 1 J ,1,1, Al ilUl,.! 1^157171185^99 227241 267 | 340 31.40 31.60 31.80 32,00 __ 11 "T-q-r I I I I I I I . I I I . 11 I I Ti r . I nrH m/z SYTOO 52.18% ^bundance 40 60

53 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) ft 5000 229 31.40 31.60 31.80 32.00 m/z 4^705 43.59% 284 " I " " 11' 111,,,, 1111111, I ' ' ' ' I ''' 'I' > I r I'' ' 11 11' 11 • " ' I'' ' ■ I I • • I p r, ■ 11, Ti/k-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 (Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

31.40 31,60 31,80 32.00 5000 m/z 41.05 36.90% 285 267 J 340 241 I I, rr+r, Uk '''I'‘''I'' I r I " 111 I i.i 11 p '' I P ''' p '' ■ i'''' I pl' 11' 11 ■n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 53 __3L40_3t60_^1J0_32j00_ m/z 73.00 30.85% 5000 285 340 73 267 129 185 241 I TTp-TTTp>T-rrpTTT7TTTTpT-rT-p-^^ T-rp-TT-q-TT '' I'' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22779.D NP091101.M Thu Oct 04 14:21:21 2001 Paae 7 NYC-WTC_000087707

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NYC-WTC_000087707Source: NYC Law Department, mirrored locally

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