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GC/MS analysis results, sample AD22919, October 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD22919 conducted on October 5, 2001, identifying other unknown compounds.

NYC-WTC_000087623–000087643

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\22919.D Vial: 9 Acq On 2 Oct 2001 9:56 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.67 0.73 ug/1 93285 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Butyl tetradecanoate (myristate) 284 C18H36O21 000000-00-0 80 Octadecanoic acid, butyl ester 340 C22H44O2: 000123-95-5 64 3 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2; 000646-13-9 59 4 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 Abundance Scan 2900 (31.667 min); 22919.D (-) Tm/z 56700 107700% 55

5000 4 73 129 285 31.40 31.60 31.80 32.00 I ,Jl.^ IF.! 71^?^ 207 241 Y i “1 pF I 11 I I fl f I I I I I j J I Kry I • I I I f I I I I i“i I I I I 11 I I I I I I j I I I I j‘ “• I I j 340 nrfnn m/z 57.00 74741% TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186; Butyl tetradecanoate (myristate) 55

5000 ,.......... 229 31.40 31.60 31.80 32.00 211 in/z 43.05 43778% , 129 284 TThTnyrri-Tp-fh-ry Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570; Octadecanoic acid, butyl ester 55. d 31.40 31.60 31.80 32.00 553 m/z 47705 34.96% 285 340 73 129 267 185 241

iiZz-> 40 60 Wn I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I'''' I I'''' I I'''' I

^bundance #48214; Octadecanoic acid, 2-methylpropyl ester 57 31.40 31.60 31.80 32.00 m/z 55.00 31.03%

553 285

‘' I'' .T a.TV.Cl..... ........ ........... ... 340 I" * ' ’ I ' ' ' ' I ' • • r I I f 1 .1 I I I I |-| I I I ytT. I I iTi I I I 1 I I p I I rp 1 . I J ri i ■ । ■ TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22919.D NP091101.M Thu Oct 04 10:03:31 2001 Page 5

NYC-WTC_000087634

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