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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088789
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial: 6 Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.64 2.71 ug/1 310285 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 80 2 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 43 3 2-Methyl-N-1-tridecene 196 C14H28 018094-01-4 35 4 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 Abundance Scan 2898 (31.643 min): 23498.D (-) pm/z 56.00 100.00% 5^

5000 4 73 129 285 I ' ' ' '7 31.40 31.60 31.80 32.00 ji I'' " I " '' I' ” ' I'''' I' I'' 340 in/z 57.00 51.04% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 5

5000 73 229 Tn/z; M 31.40 31.60 31.80 32.00 43.05 41.11%

■n/z-> 20 40 60 129 . J....... 211

I I I 11 I (I I I I ' ' " I ’ ri . I . ■ I 1 I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 284 111" ■ I" " I " '' I

Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57-

31.40 31.60 31.80 32.00 552 m/z 41.05 34.57% 285 A 7 97 129 267 i I II ,1 I.,.i r, I I ll .... ^85 340- .241 [ L rrt^ pmrTpnrTTjTTTTYTTTTp+nrY^rTTy Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21975:2-Methyl-N-1-tridecene 55. T -■---- ^3t40 - 31.60 31.80 32.00" -m/z ■ 55.00 30.61%

552 J I

27 I 83 I I I t pi1 140 168 196 I " • ‘ I • • " I' " • I p-n-TT Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280300320 340 ■ 31.40 31.60 31.80 32.00

23498.D NP091101.M Thu Oct 18 10:10:46 2001 Page 9

NYC-WTC_000088789

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NYC-WTC_000088789Source: NYC Law Department, mirrored locally

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