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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088920
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 31.64 1.54 ug/1 164390 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual Qu Butyl tetradecanoate (myristate) 284 C18H36O2: 000000-00-0 80 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 70 3 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 37 4 2-Methyl-1-tetradecene 210 C15H30 000000-00-0 32. Abundance Scan 2897 (31.640 min): 23503.D (-) m/z 56.00 100.00% 55

5000 4- 73 285 ....... Urn..... 340 31.40 31.60 31.80 32.00 I " • I" " I" " I" ’' I" " I'' " I "I m/z 57.00 51727% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) • 53

5000 229 __3r40_J1^6g_^L80_3Zp0_ 73 129 211 m/z 43775 45.75% 284 111111111111II11 ' Il' I'' ‘' I T'' 'U ■nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5(7

31,40 31.60 31.80 32.00 5000 m/ z 41.05 36.11%

7I II 285 267 J d n/z~> Abundance I'''' I'' 20 40 60 ''' I''"I 129 ' I 'I ' • I ‘ 185 241 XU ' I ' H I I . . . . I . , . . pnr 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #28775: Pentadecane, 8-methylene- 340

J ' I ' ''' I ' ' ' ' I ' ' 55 31.40 31.60 -31.80- 32.00— m/i 73 .-00—- 29.80%

553

27 I 196 224 I' " ' I • •'' I''' < 11'' > I I " " I' ‘' U n-r-p-rr- Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23503.D NP091101.M Thu Oct 18 10:28:59 2001 Page 9

’ N YC-WTC2000d88920

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NYC-WTC_000088920Source: NYC Law Department, mirrored locally

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