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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088279
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Butyl tetradecanoate (myristat Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.. 31.64 5.47 ug/1 570308 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl tetr, tecanoate (myristate) 284 C18H36O2! 000000-00-0 72 2 Octadecand'ic acid, 2-methylpropyl e 340 C22H44O21 000646-13-9 66 3 Octadaeranoic acid, butyl ester 340 C22H44O2 000123-95-5 50 4 1-H^ne, 2,5-dimethyl-_____________ 112 C8H16 006975-92-4 27 AbundancX Scan 2898 (31.643 min): 23322.D (-) Tm/z 56.00 100.00% 53

5000 4' 73 129 285

nfe-> 40 UMUW 60 80 143157171 213227241 Tyr-rrTyTTVr-pS-T TpT-rrp-rTpTTTTp-Hnry-FrTT^^

100 120 140 160 180 200 220 240 260 280 300 320 340 I 340 . ...... .. m/z 31,40 31.60 31.80 32.00 57.00 50.42% Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 31.40 31,60 31.80 32.00 211 m/z 4^/00 40.92% 284 A Ti/z-> 40 '' I' 60 80 I' " ' I'' " I' ' I' ’ " I 100 120 140 160 180 200 220 240 260 280 300 320 340 4^ Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 7 rxrrr T-r-p—r-n-p-T 31,40 31,60 31.80 32.00 5m m/ Z 41.05 34.53% 285 267 J

ntz-> 40 60 80 97..,, 129 185 I'' •' I " " I atXJL ■ I' , > 11 111 ■ I r, ■, I 100 120 140 160 180 200 220 240 260 280 300 320 340 340

^bundance #73570: Octadecanoic acid, butyl ester 53 31,40 31.60 31,80 32.00 m/z 73700 31.15%

5000 285 340 129 267 185 241 I I'''' I I ' ' ' ' I '' ' ' I I''' ' I T ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23322.D NP091101.M Mon Oct 15 10:26:08 2001 Page 10

NYC-WTC_000088279

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NYC-WTC_000088279Source: NYC Law Department, mirrored locally

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