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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088278
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heptadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.70 2.16 ug/1 224871 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 91Y 2 Tricosane 324 C23H48 000638-67-5 91 ' 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 / 4 Tetracosane 338 .C24H50 000646-31-1 90 Abundance Scan 2795 (30,697 min): 23322,D (-) m/z 56795 100.00%

43 T 71 ft 5000 85

30,40 30,60 30,80 31,00 211225239 r-TTT-p-TTn-pnn-TpnnTqprT-rTpnnT-y-rT m/z 71.10 74.00% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193: Heptadecane 57

71 5000 85 30,40 30,60 30,80 31,00 m/z 43.05 66.66% 99 J ^P'‘?7141 155169 210 240 ' I'' I' I' 1. 11'.., I,,, , 11 11 ■ 111., I,, I ' ' ' ' r ' * ' I ‘ ‘ ' I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57 l\ 71 30,40 30,60 30,80 31,00 5000 85 in/z 85.05 47.98%

99 113127141 1 I ' ' ' 183197211225 I''' ‘ I'''' I'''' I'''' I'''' I '''' I'''' I'''' I 296 r* 324 I ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- / 57 30,40 30,60 30,80 31,00 71 m/z 41.05 24.73% 5000 85

99 113. 127141155 183 211 268 296 p-rTry p-TTTp-rr-Tp •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30,40 30,60 30,80 31,00

23322.D NP091101.M Mon Oct 15 10:26:06 2001 Page 9

NYC-WTC_000088278

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NYC-WTC_000088278Source: NYC Law Department, mirrored locally

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