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GC/MS analysis results for sample AD22579, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087194
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22579.D vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heptadecane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

32.76 0.64 ug/1 105592 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Triacontane ____________________ 422 C30H62 000638-68-6 90 Abundance Scan 3020 (32.762 min): 22579.D (-) m/z 57.00 100.00% 57

43 71

5000 85

99 A ' '"l 32.40 32.60 32.80 33.00 253 I ' ' '' ' I m/z 71.00 66.88% ft I''' ‘ I'''' I'''' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 57 71

5000 85 JI ’"TT 32.40 32.60 32.80 33.00 99 m/z 47705 65776% 196 240 . 111 r 11 I. i' 1111111,,,,,, 111.,.,. ''' I ■''' I"'' I'''' I'''' I'''' I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57. 71 85 32.40 32.60 32.80 33.00 5000 m/z 85.05 47.09“% 99

I ' ' " ' I ' ' ' ' I ' ' ' '' I 268 296 I' ‘' I'''' I'''' I .................. •'•I' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5 7 32.40 32.60 32:80 33.00 71 ■mTz 41705 27.38% 5000 85

99 ..o J I jLTs I' '155169183197 I'''' I'' ‘' p''‘ I I''''' I ''' ' I' ‘' I I' ''' I'''' I'''' I 294 338 I'''' I' nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22579.D NP091101.M Tue Oct 02 11:50:19 2001 Page 8

NYC-WTC_000087194

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