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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086927
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptadecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 33.72 0.50 ug/1 63053 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual y/Heptadecane 240 C17H36 000629-78-7 94 2 Hexadecane 226 C16H34 000544-76-3 91 3 Heneicosane 296 C21H44 000629-94-7 90 4 Hexatriacontane_________________________ 507 C36H74 000630-06-8 90 (Abundance Scan 3124 (33.717 min): 22544.D (-) m/z 56.95 100.00% 57 A 43 71

5000 85

, 99 113 33.40 33.60 33.80 34.00 183 208 239 282 I . n . I T'l I i“| 1-rT I I |'"| I I i' I ' I ' I ' ' ' ' I ' ’ ' ' I ' ■p" m/z 71.00 66.58% ■tiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 <M3undance #71194: Heptadecane 4(3 57

5000 71 85 m/z 4k 33.40 33.60 33.80 34.00 43.05 I ' ' ' ' I

65.55%

nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #29267: Hexadecane c 71 V—fTCTYYYrTI.......... 33.40 33.60 33.80 34.00 253 85 m/z 85.05 48.71% I 99 226 196 -TT-y 1 ' ' ' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane ' ' I ' 57 33.40 33.60 33,80 34.00 71 m/z 41705 277^7% 85 252 99 ................ 268 ,296 ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 33,40 33.60 33.80 34.00

22544.D NP091101.M Mon Oct 01 12:59:10 2001 Page 6

NYC-WTC_000086927

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NYC-WTC_000086927Source: NYC Law Department, mirrored locally

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