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GC/MS analysis results for sample AD23839, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23839 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089366–000089384

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089381
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT3001\23839.D Vial: 13 Acq On : 31 Oct 2001 2:14 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ***************************** ** ****************** *************'^*****^ Peak Number 9 Heptadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 34.56 0.54 ug/1 129695 Chrysene-dl2 33.06 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 2 Hexadecane 226 C16H34 000544-76-3 .* 3 Heneicosane 296 C21H44 000629-94-7 91 4 Nonadecane 268 C19H40 00062’9-92-5 91 <\bundance Scan 3215 (34.556 min): 23839.D (-) jn/z 57700 100.00% 57

43 71 5000 85

99

ttZz-> “Kbundance XUM 40 60 80 100 . T. I , . 1 . j . . 120 140 169 183 I I 1' 1 , , 160 #32063: Heptadecane 207 240 2^ 1I ,, I , , , , I , , ,■! I I I 1 I I I I I I I I 180 200 220 240 260 280 300 34.20 34.40 34.60 34.80 m/ Z 71.10 64.44%

57 71 5000 85 T IK. 34.20 34.40 34.60 34.80 99 . m/ Z 43.00 63.90% tXt J I 113 127141 196 I ' ' ' ' I ' ' ' ' I 240 I ' ' • ' I ' ' ' ' I TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #29267: Hexadecane 71

?. 34.20 34.40 34.60 34.80 5000 85 Wz 85.05 47731%

99 -196- -226 prr‘TT-Y-rT-rT*Y"rT-t*T-yT*r-rT-[^^^ T)Zz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57- rfYzz ■34.20 _ 34.40'34.60 34.80 71 "inTz 41.05 21.86% 85 5000 t-

99

nZ2“> ....u.i 100 "120' '140' ieo' iso' 40 60 80 Iso' 240 260 '280 "360 ■ 84.20 34.40 34.60 34.80

23839.D NP103001.M Thu Nov 01 14:36:08 2001 Page 9

NYC-WTC_000089381

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NYC-WTC_000089381Source: NYC Law Department, mirrored locally

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