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GC/MS analysis results for sample AD23839, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23839 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089366–000089384

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089382
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3001\23839.D Vial: 13 Acq On : 31 Oct 2001 2:14 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.45 0.56 ug/1 110329 Perylene-dl2 37.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 9P 3 Nonadecane 268 C19H40 000629-92-5 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 ^bundance Scan 3312 (35.447 min): 23839.D (-) m7z 57700 100.00% 5|7

5000 85

35.20 35.40 35,60 35.80 267 I'''' I I'''' I' ‘' I m/z43.00 66.05% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane 57

85 5000 35.20 35.40 35.60 35.80 m/z 71.10 63.48%

Ti/z-> 40 JU 60 80 I'' ■' I " '' I 268 296 I '''' I ''' 11 ' 100 120 140 160 180 200 220 240 260 280 300 320 340 I " '' I'' " I

Abundance _ #49558; Heptadecane, 9-octyl-______ _ ___ 57 , . 1“. I , . . , f. , TVi t .*1 V| I 1*1 35.20 35.40 35.60 35.80 5000 85 m/z 85.05 47737)%

—141 1^- _____ 239 _ _ 310 352 Ti/z-> 4 p' I I'''' I'''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance - #71949: Nonadecane -I .| J ,! 7 J 35,20 35.40 - 35,60 - 35.80 - m/z 55.00 23.70%

5000 _85____

J , 141 . 169 224 268 y+rTTYrr+Tp+TTYTTrYpT^ 'I" " I I'''' I'''' I'''' I •n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

23839.D NP103001.M Thu Nov 01 14:36:10 2001 Page. 10

NYC-WTC_000089382

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NYC-WTC_000089382Source: NYC Law Department, mirrored locally

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