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GC/MS analysis results for sample AD23084, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23084 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087904–000087919

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0 4 01\23084.D Vial: 4 Acq On 4 Oct 2001 6:27 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★ if*******************************************************************

Peak Number 6 Heptadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.71 0.55 ug/1 88908 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

:eptadecane 240 C17H36 000629-78-7 95 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 4 Nonacosane 408 C29H60 ___ 000630-03-5 91 'Abundance Scan 3123 (33.709 min); 23084.D (-) m/z 57.00 100.00% 57 71 5m 4

Ti/z-> Abundance 40 XU 60 207227_______ '' I'''' I'' '' I'''' I'''' I' ''' I'' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #32063; Heptadecane m/z 33.40 33.60 33.80 34.00 71.10 69.36%

57

85 5000 ......................... 33.40 33.60 33.80 34.00 m/z 43.05 64.38% 196 240 I'''' I''' ’ I' .. I" I''" I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 <\bundance #42201; Heneicosane 57

' 85 33.40 33.60 33.80 34.00 5000 m/z 85.0.5 50.50%

rI Ti . I I I I I < I I I I I I I . > > I I I I ■ I 268 296 p-rrrpn-rry I'''' I I'''' I'''' I' m/z->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #49558; Hep'tadecane, ^octyl- 57 33.40 33.60 33.80 34.00 m/z 41.05 28.61% 5000 A 85

239 I 310 352 ■ I' I'' I'''' I' ‘' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

23084.D NP091101.M Tue Oct 09 12:29:42 2001 Page 6

NYC-WTC_000087916

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NYC-WTC_000087916Source: NYC Law Department, mirrored locally

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